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Chemistry 1st Paper · Classes 11-12 · Chapter 1 · 1.3

Techniques to Keep the Laboratory, Equipment and Glass Apparatus Clean.

After the experiment a reagent bottle sits on the table, a scrap of filter paper blocks the sink, and drops of water cling to the burette. None of these is a small slip. The rules for keeping a lab clean are short, and each has a reason behind it.

1. The lab, its glass and who looks after it

A school or college chemistry lab usually has two rows of long tables. Each has student desks and a shelf for reagent bottles, plus a water pipe, a basin and a gas pipe for the Bunsen burners. Chemicals live in their own cupboards or shelves. Glassware, and metal and plastic apparatus, each go in separate cupboards too.

The pipette, burette and conical flask are made of pyrex glass, so heat does not break them easily. After washing a burette, pipette, conical flask or funnel, drops of water sticking to the glass tell you it is not clean yet.

The lab is run by the lab assistant, the demonstrator and the chemistry teacher in charge. Even so, every student must leave the lab clean after using it.

2. Where waste and bottles go

During an experiment, broken glass tube, used filter paper and torn paper must never go into the water sink. Put them in the dustbin kept at its fixed place in the lab.

After use, a reagent bottle goes back to its place on the shelf and does not stay on the table. At the end of the experiment, clean the glass tubes you used, leave them on the stand to dry, then arrange them on the table.

See first where each thing goes, and what follows when it goes in the wrong place.

the waste a thing, then a place

Sink or dustbin?

Now put them all in their places in one go.

sort them Pick a chip, then a bin.

Where does each go?

Pick up a chip, then drop it in a bin. For anything lying in the sink, remember it should not be there.

3. The chemical balance

The Class 11-12 experiments use various glassware, the chemical balance, the Bunsen burner and the thermometer. Career-oriented chemistry adds a pressure canning machine, cans and a cream machine.

The chemical balance weighs pure chemicals accurately. It is a valuable instrument, so learn the method from your teacher before you use it.

Three jobs after using it: wipe the pan with tissue paper or flannel cloth, put the weights back in their places in the weight box, and close the door of the balance box.

4. Washing glassware

An experiment starts with clean glassware. Dirty or opaque glassware cannot be used for a chemical experiment. Usually a wash in tap water is enough.

For oily matter, especially in a burette stopcock, use the chromic acid mixture (K₂Cr₂O₇ and concentrated H₂SO₄) kept in a bottle. Handle it carefully, with gloved hands. Ammonia solution is also used to clean glass apparatus.

To clean a test tube, hold it in your left hand under the tap and work the brush with your right.

Solutions of coloured substances such as iron salts, copper salts, KMnO₄ and K₂Cr₂O₇ stick to the inside of a test tube if left, and take a long time to clean later. So wash it right after use.

Glass tells you itself whether it is clean. Run water down three burettes, then wash each to suit its dirt.

the water test run water

Drops or a thin film?

Now test the book's rule on four short cases. The first is about a burette.

is it clean

Is it clean?

After washing, drops of water cling to the burette. What does it show?

The second is about a coloured solution.

is it clean

When colour sticks

What happens if a KMnO₄ solution is left unwashed in a test tube?

The third is about the burette stopcock.

is it clean

An oily stopcock

What cleans the grease in a burette stopcock?

The last is about the balance pan.

is it clean

The balance pan

What wipes the balance pan?

Short facts blur together when read once. Answer each of these eight cards in your head, then turn it over.

quick recall Think, then tap.

Quick recall

QuestionWho runs the lab?
AnswerLab assistant, demonstrator, chemistry teacher
QuestionWhat is the chemical balance for?
AnswerAccurate weight of pure chemicals
QuestionThe pan is wiped with?
AnswerTissue or flannel
QuestionPipette and burette are which glass?
AnswerPyrex
QuestionWhere do reagent bottles go?
AnswerOn the shelf
QuestionTwo solutions that clean glass?
AnswerChromic acid mixture, ammonia
QuestionBrush in which hand?
AnswerThe right hand
QuestionWhich coloured substances stick?
AnswerFe, Cu salts, KMnO₄, K₂Cr₂O₇

5. Check yourself

The first question is in the exam's style.

check yourself pick one answer

Question 1

What is a test tube ordinarily washed with?

For the second, recall the book's rule.

check yourself pick one answer

Question 2

The following are used to clean glass apparatus:

i. Ammonia solution
ii. Acetone, to remove oil and grease
iii. Concentrated phosphoric acid

Think the last one through before you choose.

check yourself pick one answer

Question 3

After washing a burette, drops of water cling to its inner wall. What does this show?

The whole note on seven cards.

cut from the note tap to turn over

Seven cards

QuestionWhat do drops of water clinging to a washed burette or pipette show?
AnswerThey are not clean
QuestionWhere are broken glass tube and used filter paper thrown?
AnswerIn the dustbin, not in the water sink
QuestionWhere is a reagent bottle kept after use?
AnswerOn the shelf in its place, not on the table
QuestionWhat are the three things to do after using the balance?
AnswerWipe the pan with tissue or flannel, put the weights in place, keep the box door closed
QuestionWhich mixture cleans oily matter in a burette stopcock?
AnswerThe chromic acid mixture (K₂Cr₂O₇ and concentrated H₂SO₄), with gloved hands
QuestionSolutions of which coloured substances stick to an unwashed test tube?
AnswerIron salts, copper salts, KMnO₄, K₂Cr₂O₇
QuestionBesides the chromic acid mixture, which solution cleans glass apparatus?
AnswerAmmonia solution

Source: Chemistry 1st Paper, Classes 11-12 (NCTB), Chapter 1 “Safe Use of the Laboratory”, section 1.3.