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Chemistry 1st Paper · Classes 11-12 · Chapter 1 · 1.2

Safe Techniques to Use Glass Apparatus.

The thing in the lab that breaks most easily is also the sharpest once it has broken. This note covers how glass apparatus breaks, what keeps your hand safe before it does, and which glass can take the flame.

1. How glass apparatus breaks

Lab glassware includes the test tube, beaker, funnel, conical flask, measuring flask, pipette, burette, measuring cylinder, round-bottom flask, glass rod, glass tube and Liebig condenser.

All of it breaks easily on impact. Broken glass is sharp and can cut the skin and make it bleed.

There are six risks: knocking the tap or basin while washing, too much pressure fitting a tube in a holder, too much pressure in a clamp, heating with water on the outer wall, pushing a tube or thermometer into a stopper, and a fall from a height. Match the pairs.

match them match the six pairs

Which job, which risk?

Pick up a job, then drop it in the box of the risk it brings.

2. Fitting a tube into a stopper

Pushing a glass tube into a bored cork or rubber stopper is one of the riskier jobs. Wrap both the tube and the stopper in a towel and press the tube through the hole, so that if it snaps your hand stays uncut. If it will not go in, enlarge the hole and wet it with water or glycerine.

The towel and the wetting are two small jobs. Leave one out, press the tube, and see what happens.

on the bench press

A glass tube into a stopper

Now put the steps in order.

in order protect the hand first

Put the steps in order

What comes first, so that a snapped tube cannot cut your hand?

3. Soft glass and pyrex

By the glass used, lab glassware is of two kinds: soft glass, and hard or pyrex glass. Soft glass items are the glass tube, beaker, watch-glass, funnel, reagent bottle and Liebig condenser.

Soft glass melts and softens easily in a Bunsen flame; it takes little heat. It is not brown or very transparent.

Pyrex items: beaker, conical flask, pipette, burette, measuring cylinder, volumetric flask, round-bottom flask and distillation flask. Pyrex stands high heat and is very strong, so strong heating, round-bottom flasks for preparations, distillation flasks and vacuum-filtration apparatus are made of it.

Notice that the beaker is in both of the book's lists, so there is a third box for it below.

sort them recall the book's lists

Which glass is it?

Pick up a chip, then drop it in a box.

Chemically, pyrex is made from a mixture of zinc oxide and barium borosilicates, and soft glass from a mixture of sodium and calcium silicates. So to heat a mixture or solution, take a pyrex beaker or conical flask.

4. Check yourself

The first question is in the exam's style.

check yourself pick one answer

Question 1

Which glass is used to make a burette and a pipette?

For the second, work out which glass it is.

check yourself pick one answer

Question 2

The possible causes of breaking glass apparatus are-

i. Hitting the basin while washing
ii. Applying too little pressure when fixing in a clamp
iii. Heating on a Bunsen burner while water is on the outer wall

The last one is a final reminder.

check yourself pick one answer

Question 3

What is done to avoid cutting the hand while pushing a glass tube into a bored cork?

The whole note on seven cards.

cut from the note tap to turn over

Seven cards

QuestionWhat is the risk of heating glass while water is on its outer wall?
AnswerIt is one of the causes of breaking the glass
QuestionWhat is wrapped round when pushing a glass tube into a stopper, and why?
AnswerA towel, so that broken glass does not cut the hand
QuestionWhat is done if the glass tube does not enter the stopper hole easily?
AnswerEnlarge the hole and wet it with water or glycerine
QuestionWhat happens to soft glassware heated in a Bunsen flame?
AnswerIt melts and softens easily because it withstands little heat
QuestionWhich glass are the pipette, burette and conical flask made of?
AnswerPyrex (hard) glass
QuestionChemically, what is pyrex glass made of, and what is soft glass made of?
AnswerPyrex: zinc oxide and barium borosilicates; soft: sodium and calcium silicates
QuestionFor heating a solution, a beaker or conical flask of which glass is used?
AnswerHard or pyrex glass

Source: Chemistry 1st Paper, Classes 11-12 (NCTB), Chapter 1 “Safe Use of the Laboratory”, section 1.2.